Synthesis and Characterization of CaF2 NPs with Co-precipitation and Hydrothermal Method
Author:
, , , , , , ,Year
: 2011
Abstract: Abstract
We used CaCl2 and NH4F from Merck Company for synthesis CaF2 NPs. We synthesized CaF2 Nanoparticales
(NPs) using Co-precipitation and hydrothermal method successfully. The synthesized NPs were characterized by X-ray
diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, Transmission Electron Microscopy (TEM), Scanning
Electron Microscopy (SEM), UV-Vis spectroscopy and Photoluminescence (PL) techniques. The XRD results indicated
the formation of CaF2 NPs with Cubic phase and the crystallite size is estimated using Scherrer’s to be in the range
20–27nm for the powders prepared by co-precipitation and 20–31nm for hydrothermal methods, respectively. TEM
images revealed the grains have almost spherical shape. Optical absorption spectrum shows a strong absorption edge
at about 300nm.
We used CaCl2 and NH4F from Merck Company for synthesis CaF2 NPs. We synthesized CaF2 Nanoparticales
(NPs) using Co-precipitation and hydrothermal method successfully. The synthesized NPs were characterized by X-ray
diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, Transmission Electron Microscopy (TEM), Scanning
Electron Microscopy (SEM), UV-Vis spectroscopy and Photoluminescence (PL) techniques. The XRD results indicated
the formation of CaF2 NPs with Cubic phase and the crystallite size is estimated using Scherrer’s to be in the range
20–27nm for the powders prepared by co-precipitation and 20–31nm for hydrothermal methods, respectively. TEM
images revealed the grains have almost spherical shape. Optical absorption spectrum shows a strong absorption edge
at about 300nm.
Keyword(s): Keywords: Nanoparticle,Co-precipitation,Hydrothermal,
Photoluminescence (PL),Scherrer’s formula
Collections
:
-
Statistics
Synthesis and Characterization of CaF2 NPs with Co-precipitation and Hydrothermal Method
Show full item record
| contributor author | ام الفجر نخعی | en |
| contributor author | ناصر شاه طهماسبی | en |
| contributor author | محمود رضائی رکن آبادی | en |
| contributor author | احمد کمپانی | en |
| contributor author | fajri nakhaei | fa |
| contributor author | Nasser Shahtahmassebi | fa |
| contributor author | Mahmood Rezaee Roknabadi | fa |
| contributor author | Ahmad Kompany | fa |
| date accessioned | 2020-06-06T14:37:06Z | |
| date available | 2020-06-06T14:37:06Z | |
| date issued | 2011 | |
| identifier uri | https://libsearch.um.ac.ir:443/fum/handle/fum/3404237 | |
| description abstract | Abstract We used CaCl2 and NH4F from Merck Company for synthesis CaF2 NPs. We synthesized CaF2 Nanoparticales (NPs) using Co-precipitation and hydrothermal method successfully. The synthesized NPs were characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), UV-Vis spectroscopy and Photoluminescence (PL) techniques. The XRD results indicated the formation of CaF2 NPs with Cubic phase and the crystallite size is estimated using Scherrer’s to be in the range 20–27nm for the powders prepared by co-precipitation and 20–31nm for hydrothermal methods, respectively. TEM images revealed the grains have almost spherical shape. Optical absorption spectrum shows a strong absorption edge at about 300nm. | en |
| language | English | |
| title | Synthesis and Characterization of CaF2 NPs with Co-precipitation and Hydrothermal Method | en |
| type | Journal Paper | |
| contenttype | External Fulltext | |
| subject keywords | Keywords: Nanoparticle | en |
| subject keywords | Co-precipitation | en |
| subject keywords | Hydrothermal | en |
| subject keywords | Photoluminescence (PL) | en |
| subject keywords | Scherrer’s formula | en |
| journal title | Journal of Nanomedicine and Nanotechnology | fa |
| pages | 5-Jan | |
| journal volume | 2 | |
| journal issue | 5 | |
| identifier link | https://profdoc.um.ac.ir/paper-abstract-1024380.html | |
| identifier articleid | 1024380 |