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RISA new phosphorothioic triamide structure: P(S)[NHCH2C6H5]3
The structure of N,N',N"-tribenzylphosphorothioic triamide, C21H24N3PS, (I), and analysis of the bond-angle sums at the N atoms for this compound, and for 74 structures with a P(S)[N]3 skeleton and the N atom in a ...
Analysis of S—P—N and N—P—N angles in phosphorothioic triamides
The S—P—N and N—P—N bond angles have been analyzed in 30 phosphorothioic triamides structures (having a P(S)[N]3 skeleton) deposited in the Cambridge Structural Database (CSD, version 5.34, May 2013 update) and a new structure reported...
The first phosphorothioic triamide–mercury (II) complex with a P(S)[N]3–based ligand: Synthesis and crystal structure of PS(NC5H10)3 and [Hg{P(S)(NC5H10)3}Cl2]2
The synthesis, spectral study and X-ray crystal structure of PS(NC5H10)3 phosphorothioic triamide (compound 1) and its dinuclear mercury(II) complex, [Hg{P(S)(NC5H10)3}Cl2]2 (compound 2), were investigated. The structure 2 is the first...
Hirshfeld surface analysis of two new phosphorothioic triamide structures
Hirshfeld surfaces and two-dimensional fingerprint plots are used to analyse the intermolecular interactions in two new phosphorothioic triamide structures, namely N,N',N"-tris(3,4-dimethylphenyl)phosphorothioic triamide acetonitrile hemisolvate, P...
The first X-ray crystal structure of a mercury-II- complex with an SP-N-3-based ligand: Synthesis and crystal structure of SP-NC5H10-3 and [Hg{SP-NC5H10-3}Cl2]2
The synthesis, spectral characteristics -IR and NMR-, elemental analysis and X-ray crystal structure of phosphorothioic triamide SP-NC5H10-3 -1- and its dinuclear mercury-II- complex [Hg2-μ-Cl-2-Cl-2{SP-NC5H10-3}2] -2- were investigated. A survey...
Two new thiophosphoramide structures: N,N',N"-tricyclohexylphosphorothioic triamide and O,O'-diethyl (2-phenylhydrazin-1-yl)thiophosphonate
The compound N,N',N"-tricyclohexylphosphorothioic triamide, C18H36N3PS or P(S)[NHC6H11]3, (I), crystallizes in the space group Pnma with the molecule lying across a mirror plane; one N atom lies on the mirror plane, whereas ...