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RISSynthesis and Crystal Structure of P(O)(Cl)[N(CH3)(CH2C6H5)]2
Synthesis and Crystal Structure of P(O)(Cl)[N(CH3)(CH2C6H5)]2...
Synthesis, characterization and crystal structure of a silver(I) complex containing AMTT - (AMTT=4-amino-5-methyl-2H-1,2,4-triazole-3(4H)-thione)
The reaction of 4-amino-5-methyl-2H-1,2,4-triazole-3(4H)-thione with AgNO3 in methanol led to the complex [Ag(ATT)2]NO3 (2). 2 was characterized by elemental analyses, IR, 1HNMR and Raman spectroscopy as well as single-crystal X-ray diffraction...
Synthesis and Crystal Structure of a New Hydrated Phosphinate Salt, [(C6H5CH2)2NH2][(C6H5)2P(O)(O)].H2O
of 116.38(9)˚ for the O–P–O angle and the lowest angle of 102.74(10)˚ for the C–P–C angle. The most characteristic feature of the cation is the open C–N–C angle (of 113.50(17)˚). In the crystal structure, the cations, anions and water molecules...
Synthesis, spectroscopic characterizationand crystal structure and of N-(bis-isopropylamino)phosphoryl-3-nitro benzamide
Synthesis, spectroscopic characterizationand crystal structure and of N-(bis-isopropylamino)phosphoryl-3-nitro benzamide
Vahid Rezaei 1, Mehrdad Pourayoubi1
Chemistry Department, Ferdowsi University of Mashhad, Mashhad...
Synthesis and characterization of some new phosphoramide and thiophosphoramide derivatives: crystal structure of CHCl2C(O)NHP(O)[NHCH2CH2CH3]2
length (of 1.6962(16) Å) is longer than the two other P―N bonds (1.6201(16) and 1.6257(18) Å). In the crystal structure, molecules are aggregated in a one-dimensional arrangement parallel to the plane (1–10) in the direction perpendicular to the (110...
Crystal Structure of Bis(dipropylammonium) Tetrachloro-Dimethyl-Tin(IV)
-aminopyridinium) dimethyl-tetrachloro-tin(IV) (CSD refcode GEKDEF; Valle et al., 1988)4. Here, the structure of a new organotin(IV) compound with formula [(C3H7)2NH2+]2[Sn(CH3)2Cl4]–2 is reported. The crystal belongs to space group P2(1)/n with cell dimensions a...
Crystal growth and intramolecular hydrogen bond effects on activity of a novel Schiff base ligand: An experimental and theoretical approach
Reaction of thiosemicarbazide with alkyl halides produce isothiosemicarbazides which in condensation reactions with aldehydes or ketones could yield isothiosemicarbazones. A new tridentate Schiff base compound, salicylaldehyde ...
A new phosphoric triamide structure: (CF3C(O)NH)P(O)(NHC6H4-4-CH3)2
The synthesis, spectroscopic characterization (1H-, 13C-, 31P-, 19F-NMR, IR and mass) and single crystal X-ray diffraction analysis of (CF3C(O)NH)P(O)(NHC6H4-4-CH3)2 were investigated. The compound was crystallized in the chiral space group P21...