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RISSynthesis and Crystal Structure of P(O)(Cl)[N(CH3)(CH2C6H5)]2
Synthesis and Crystal Structure of P(O)(Cl)[N(CH3)(CH2C6H5)]2...
Synthesis, characterization and crystal structure of a silver(I) complex containing AMTT - (AMTT=4-amino-5-methyl-2H-1,2,4-triazole-3(4H)-thione)
The reaction of 4-amino-5-methyl-2H-1,2,4-triazole-3(4H)-thione with AgNO3 in methanol led to the complex [Ag(ATT)2]NO3 (2). 2 was characterized by elemental analyses, IR, 1HNMR and Raman spectroscopy as well as single-crystal ...
Synthesis and Crystal Structure of a New Hydrated Phosphinate Salt, [(C6H5CH2)2NH2][(C6H5)2P(O)(O)].H2O
of 116.38(9)˚ for the O–P–O angle and the lowest angle of 102.74(10)˚ for the C–P–C angle. The most characteristic feature of the cation is the open C–N–C angle (of 113.50(17)˚). In the crystal structure, the cations, anions and water molecules...
Synthesis, spectroscopic characterizationand crystal structure and of N-(bis-isopropylamino)phosphoryl-3-nitro benzamide
Synthesis, spectroscopic characterizationand crystal structure and of N-(bis-isopropylamino)phosphoryl-3-nitro benzamide
Vahid Rezaei 1, Mehrdad Pourayoubi1
Chemistry Department, Ferdowsi University of Mashhad, Mashhad...
Synthesis and characterization of some new phosphoramide and thiophosphoramide derivatives: crystal structure of CHCl2C(O)NHP(O)[NHCH2CH2CH3]2
length (of 1.6962(16) Å) is longer than the two other P―N bonds (1.6201(16) and 1.6257(18) Å). In the crystal structure, molecules are aggregated in a one-dimensional arrangement parallel to the plane (1–10) in the direction perpendicular to the (110...
Crystal Structure of Bis(dipropylammonium) Tetrachloro-Dimethyl-Tin(IV)
The property of organotin compounds, R2SnX2 (X = halogen), as Lewis acids has been utilized to prepare tetrahalodiorganoastannates, [R2SnX4]–2.1 A search of the Cambridge Structural Database (CSD) shows that 17 structures ...
Crystal growth and intramolecular hydrogen bond effects on activity of a novel Schiff base ligand: An experimental and theoretical approach
Reaction of thiosemicarbazide with alkyl halides produce isothiosemicarbazides which in condensation reactions with aldehydes or ketones could yield isothiosemicarbazones. A new tridentate Schiff base compound, salicylaldehyde ...
The First Principle Studies Of Band Structure Calculations Of MgAl2O4 and 2H-SiC UsingPseudopotential Approaches
We have studied the band structure properties
of 2H-SiC in crystal structure and MgAl2O4 in closepacked
face-centered structure. In our calculations we
have adopted a pseudopotential approach based on the...
Synthesis, Spectroscopic Study and Crystal Structure of a New Amidophosphonate, (C6H5O)2P(O)(NHCH(CH3)(C2H5))
The crystal structure of diphenyl (2-butylamido) phosphonate has been determined. This crystal belongs to the space group P21/c, and the asymmetric unit of the structure is composed of one complete molecule. The P atom has a distorted tetrahedral...
Synthesis and Characterization of N-dichloroacetyl-N’,N’’ (cyclohexyl methyl) phosphoric triamide
Following our previous works about phosphorus compounds containing C(O)NHP(O) moiety such as P(O)[NHC(O)C6H4(4-NO2)][NHC6H11]2, we report here on the synthesis of a new phosphoramidate, CCl2HC(O)NHP(O)[N(CH3)(C6H11)]2. ...